Synthesis and characterization of nanocrystalline hydroxyapatite from natural bovine bone
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A Ruksudjarit, K Pengpat, G Rujijanagul…
Current applied …, 2008
Elsevier
Nanocrystalline hydroxyapatite (HA) powder was synthesized from natural bovine bone by a vibro-milling method. The bovine bone had been deproteinized by hot water before it was calcined at 800° C for 3h. The resulting product was crushed into small pieces and milled in a ball mill pot for 24h. After that the powders were ground by the vibro-milling method with various milling times. Characteristics of the powders were then investigated by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy …